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Analytical Quality by Design (AQbD) for Developing a Validated High-Performance Thin Layer Densitometry Method for Estimating Mangiferin in Human Plasma
Rajneet Kaur Khurana, Atul Jain, OP Katare, Bhupinder Singh

Analytical methods are highly vital at every stage of the product development starting from characterization of drug substance to its
estimation in dosage form, biological samples and stability studies. Development of analytical methods require complete understanding of the method variables to attain the superior method performance

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TGA/IST16/GC/MS coupling : an advanced technique for LLDPE structure interpretation
Tiffany Marre1 ; Axel Bart1 ; Alain Delauzun1 ; Xavier Cardot1 ; Ronan Cozic1 ; Olivier Boyron2 ; Christophe Boisson2

An innovative TGA/IST16/GC/MS coupling is presented.

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Combined Use of Rheometry and GPC/SEC for Characterising Ionic Polysaccharides
John Duffy, Bernd Schaefer, Bert Postma

This poster shows how Rheometry and GPC can be complementary tools for characterising the behaviour of polysaccharides in solution

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An Alternative to Direct Probe: Pyroprobe Coupled to High Resolution Time-of-Flight Mass Spectrometry
Jonathan D. Byer, Joe Binkley, Karen Sam, Jeff Patrick

Direct Pyroprobe is not a substitute for direct probe, but there is some overlap, as well as additional functionality. Direct probes coupled to LECO Pegasus instruments provide unique features:
– Time-of-flight mass spectra which shows little-to-no spectral skewing
– Automatic peak finding and spectral deconvolution for better identification
– Pegasus HT has a very low maintenance source which is beneficial for direct analysis techniques

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A Reduced Workflow Solution for the Analysis of Gamma-Hydroxybutyrate (GHB) in Human Hair Samples Via an Automated Bead Mill as a Precursor to GCxGC-TOFMS and GC-HRT
Brittany M. Watt, David E. Alonso, Joe Binkley, Jeff Patrick, Frank A. Kero, Victor Vandell, Elena Gairloch, Brad Nolt, Tom Enzweller, Rhys Jones, Lee Williams, Karen S. Scott

- The Biotage Bead Ruptor 24 was effective in pre-treating hair samples prior to the extraction procedure.
- The enhanced chromatographic resolution of GCxGC-TOFMS and high resolving power of GC-HRT minimized interferences and facilitated accurate analysis of GHB in hair.

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A FastGC Proton-Transfer-Reaction Quadrupole Ion Guide Time-of-Flight (PTR-QiTOF) Mass Spectrometer
Alfons Jordan1, Lukas Märk1, Jens Herbig1, Christian Lindinger1, Rene Gutmann1, Lukas Fischer1, Eugen Hartungen1, Simone Jürschik1, Gernot Hanel1, Philipp Sulzer1, Tilmann D. Märk1,2

In order to identify and quantify isomeric compounds independently in real-time, we introduce a novel approach where we integrate a fast GC column (“fastGC”) into a PTR-QiTOF instrument. The outstanding sensitivity of the new PTR-QiTOF (up to 4,700 cps/ppbv) is crucial for applications where time per analysis is limited, e.g. nosespace in food and flavor research. Particularly, in these fields the chemical environment is normally very complex so that a high selectivity is essential as well.

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Capillary Electrophoresis Coupled with Micro Free Flow Electrophoresis for High Speed Two Dimensional Separations of Biological Samples
Alexander C. Johnson, Michael T. Bowser

We propose using micro free flow electrophoresis (µFFE) as a solution to the under sampling problem.

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Analysis of Polymers, Additives and Contaminates in Medical Devices using Pyrolysis-GCMS
Gary Deger

Pyrolysis GC-MS is a standard technique used to analyze industrial polymers. This poster will show the use of multiple temperature ramps to analyze for additives and contaminants, in addition to polymer identification, in several medical devices.

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An investigation into the effects of aging on automotive bumper samples by xylene soluble flow injection polymer analysis (XS-FIPA)
Bassem Sabagh, Wei Sen Wong, Bernd Tartsch

This poster describes the use of flow injection polymer analysis (FIPA) as an analytical tool for xylene soluble (XS) determination with quick and easy simultaneous measurements of molecular weight (MW), intrinsic viscosity (IV) and XS%. The technique was applied to automotive bumper samples which had undergone an aging test. The results from the XS-FIPA technique highlight the differences caused by the aging process.

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Showing Results 21 - 30 of 129
Scientific News
How Cloud Connectivity Can Combat the Reproducibility Crisis
This infographic explains the reproducibility crisis, and how cloud connectivity can help overcome this problem.
Simplifying Drug Development
Scientists have for the first time revealed the nanostructure of the mesoporous magnesium carbonate Upsalite® and controlled pore size without organic molecules as templates or swelling agent.
Two New Carcinogens Found in E-cig Vapor
Berkeley Lab study identifies two additional carcinogens not previously reported in e-cigarette vapor.
Quantifying Water Content in Solid Pharma Drugs
UTA chemists devise cheaper, faster, more accurate, automated method to quantify water content in solid pharmaceutical drugs.
Core-Shell Columns in HPLC: Food Analysis Applications
Explore the most recent applications of core-shell columns in food analysis.
Review of the Analysis of Haemoglobin A1c for Diabetes Diagnostics
This paper aims to clarify methods, units, quality requirements, reference and cutoff limits for hemoglobin A1c (HbA1c) and ratio of blood glucose/HbA1c on the basis of the results from Finnish quality control surveys by comparing them to the literature.
Determination of 13 Organic Toxicants in Human Blood
Researchers have utilised liquid-liquid extraction coupling HPLC-MS/MS to identify and quantify organic toxicants in human blood.
Massive Helium Discovery a "Game Changer" for Medical Industry
A new development is gas exploration has yielded the discovery of a huge helium gas field, which could help relieve the dwindling supply.
Making Metabolite Identification More Efficient
Metasense combines the industry's most-comprehensive metabolic transformation prediction with efficient analysis of LC/MS analytical measurements to identify, visualize, and report chemical biotransformations.
ASMS 2016: Targeting Mass Spectrometry Tools for the Masses
The expanding application range of MS in life sciences, food, energy, and health sciences research was highlighted at this year's ASMS meeting in San Antonio, Texas.
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