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LC-MS/MS METHOD FOR THE QUANTIFICATION OF PITOFENONE IN HUMAN PLASMA
B.M. Gurupadayya, S. Sharfuddin and R.S. Chandan

We developed LCMS/MS bioanalytical method for quantitative estimation of Pitofenone HCl in plasma is simple, sensitive, accurate, precise, and selective. Percentage recovery shows that the method is free from interference of matrix. The analytical method presented here has proved to be useful for investigation of the characteristics of Pitofenone in human plasma in pharmacokinetic and pharmacogenetic studies.

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Validation of HPLC analytical method for determination of biogenic amines in agricultural products
Hyeock Yoon, Jae-Hyung Mah

An analytical method was validated for the quantitative determination of biogenic amines (BA) in agricultural products. The validation results fulfill AOAC criteria and recommendations. This method has been applying to analyze BA in agricultural products for a total dietary survey in Korea.

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Non-target Screening of Contaminants in Paper-paperboard for Food Contact Materials
Lukas Vapenka*, Adam Vavrous**, Lenka Votavova*, Kristina Kejlova**, Jaroslav Dobias*, Jitka Sosnovcova**

The aim of this work was non-targeted screening of xenobiotics in paper and paperboard packaging materials used for food packaging in the Czech Republic.

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Development of an Analytical Strategy for Simultaneous Determination of Multiple Contaminants in Paper Food Packaging
Adam Vavrouš (1), Lukáš Vápenka (2), Kristina Kejlová (1), Jitka Sosnovcová (1), Dagmar Jírová (1)

We developed a method for simultaneous determination of polycyclic aromatic hydrocarbons, polyfluorinated compounds, ink photoinitiators, phthalates and bisphenols in paper food packaging employing GC–MS/MS and HPLC–MS/MS.

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METHOD DEVELOPMENT FOR THE SIMULTANEOUS DETERMINATION OF METHYLMERCURY AND INORGANIC MERCURY IN SEAFOOD
Sergio Carneado, Ariane V. Zmozinski, Carmen Ibáñez-Palomino, Àngels Sahuquillo, José Fermín López-Sánchez, Márcia M. da Silva

This work reports the method development for the simultaneous determination of methylmercury (MeHg+) and inorganic mercury (iHg) species in seafood. The study focused on the extraction and quantification of MeHg+ by liquid chromatography coupled to on-line UV irradiation and cold vapour atomic fluorescence spectroscopy (LC-UV-HG-AFS), using HCl 4 mol L-1 as extractant agent.

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Microextraction techniques combined with X-ray fluorescence spectrometry for determination of different metal ions in water
Karina Kocot (a), Beata Zawisza (a), Eva Marguí (b), Ignasi Queralt (c), Rafal Sitko (a)

In present work new preconcentration procedures combining microextraction techniques and X-ray fluorescence spectroscopy were developed. Proposed methodologies are promising tools for multielemental analysis enabling detection of natural pollutants in different water samples.

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Analysis of Low Levels of Bisphenol A (BPA) in Canned Broths
Ken G. Espenschied, Michael Ye, Olga I. Shimelis, and Christine Dumas

Bisphenol A (BPA) is a primary monomer used in the manufacture of many plastics and epoxies. Some of these plastics are used as beverage containers and as liners and sealants for metal food containers. Because of BPA’s potential to act as an endocrine disrupter at low concentrations in humans, regulations have been enacted regarding BPA concentrations in food and beverages sold for human consumption.

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Fast and Efficient Analysis of Polynuclear Aromatic Hydrocarbons in Edible Oils Using Dual-Layer SPE
Christine Dumas and Katherine Stenerson

A new dual-layer cartridge for the efficient extraction of PAHs from edible oils

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Total Phenolics and Beta-1,3-Glucans Extracted from Medicinal Mushrooms (Ganoderma lucidum, Inonotus obliquus, and Phellinus linteus)
Jaecheol Kim, Kiuk Lee, Keum Taek Hwang(1), Gichun Yoo(2)

This study was to analyze the total phenolics, beta-glucans, and beta-1,3-glucans in water extracts of three medicinal mushrooms (Ganoderma lucidum(GL), Inonotus obliquus(IO), and Phellinus linteus(PL)) under different extraction conditions.

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Application of Central Composite Design (CCD) for the Optimization of Ultrasound-assisted Extraction (UAE) of Phenolics from Corn (Zea mays)
Widiastuti Setyaningsih, 1,2 Erwan Duros, 3 Ceferino Carrera, 4 Miguel Palma, 2 Carmelo G. Barroso 2

A new Ultrasound-assisted Extraction (UAE) of phenolic compounds from corn (Zea mays) has been optimized by means of chemometrics tool. The proposed method was validated and successfully applied to the analysis of phenolics content in several corn cultivars.

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Showing Results 1 - 10 of 118
Scientific News
Cells Build 'Cupboards' To Store Metals
Lawrence Livermore researchers have discovered that cells of the alga Chlamydomonas Reinhardti build a “pantry” to store metal and maintain equilibrium.
Non-Gluten Proteins as Targets of Immune Response to Wheat in Celiac Disease
The results were reported online in the Journal of Proteome Research.
Turkeys may be Lifesavers
Antibiotic to target staph infections, strep, comes from good bacteria in turkeys.
Did You Hear The One About The Two Businessmen On A Plane?
EquipNet’s vision ‘to revolutionize the way companies manage their surplus assets’ was first conceived at 30,000 feet somewhere between Chicago and Boston in 1999. Here we learn more about the company's first 15 years.
Proteomics for Systems Toxicology
MS-based proteomics is maturing into a robust technology for the measurement of proteome-wide exposure effects.
Charge-Tagged Proline-Based Organocatalyst for Mechanistic Studies Using ESI-MS
In a comparative continous flow ESI-MS study, researchers use a new charged catalyst and neutral L-proline to investigate the proline-catalyzed inverse crossed aldol reaction of aldehydes with diethyl ketomalonate.
Could Non-gluten Proteins Play a Role in Celiac Disease?
Scientists are reporting in ACS’ Journal of Proteome Research that people with the disease also have reactions to non-gluten wheat proteins.
Mass Spec Sample Prep Cut From Days to Minutes
The method, developed by Livermore scientists, accommodates liquid samples and bypasses the graphitization process, enabling sample preparation and analysis in minutes.
LLNL, UC Davis Partner to Personalize Cancer Medications
With a $7.8 million, five-year grant from the NIH researchers are utilizing accelerator mass spectrometry for cancer research.
Novel Solutions to Fight the Obesity Gene
Potent inhibitors a potential new class of anti-obesity drugs that target one of the most common genetic causes of obesity.
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