Latest Posters
Poster
High Performance Time-of-Flight Mass Spectrometry for Comprehensive Petroleum Analysis
High Resolution GC-TOFMS and GC×GC-TOFMS are useful for a non-target comprehensive characterization of petroleum through a petroleomic approach, and can also provide targeted analysis of chemical markers.
High Resolution GC-TOFMS analysis with high resolution and high mass accuracy is crucial for identification of crude oil and asphaltene pyrolysis products by unequivocal chemical formula assignment, with enhancement of sensitivity and selectivity.
High Resolution GC-TOFMS analysis with high resolution and high mass accuracy is crucial for identification of crude oil and asphaltene pyrolysis products by unequivocal chemical formula assignment, with enhancement of sensitivity and selectivity.
Poster
Non-Target and Post-Target Analysis of Organic Environmental Contaminants in Suspended River Sediments
Thermal desorption coupled to GC×GC-TOFMS and GC-HRT were effective tools for enhancing the number of compounds identifiable in suspended sediment without wet chemistry. GC×GC-TOFMS provides high chromatographic resolution for unknown identification with 2D deconvolution and mass spectral library database searching. GC-HRT provides high mass resolution and selectivity for unknown identification with High Resolution Deconvolution™.
Poster
Characterization of Complex Forensic Samples by Gas Chromatography--High Resolution Time-of-Flight Mass Spectrometry
Proper sample preparation is critical for the analysis of complex samples. GC-HRT provides high quality, accurate mass data for:
-Spectral similarity searches (NIST, Wiley, etc.)
-Formula determination (fragment, molecular, and adduct ions)
-Spectral similarity searches (NIST, Wiley, etc.)
-Formula determination (fragment, molecular, and adduct ions)
Poster
Characterization of Metabolites From Medicago truncatula Using Gas Chromatography Mass Spectrometry—Addressing the Knowns and Unknowns Using High Resolution Time-of-Flight
Analyses of the M. truncatula extracts were performed, and data processing focused on qualitative analyses. This provided the opportunity for known analyte verification and unknown identification in a meaningful matrix and the demonstration of the key attributes and benefits of GC-HRT.
Poster
Comparing Additives and Other Extractables From Primary and After-Market Cell Phone Cases by High Resolution Gas Chromatography Time-of-Flight Mass Spectrometry
High resolution GC-TOFMS on the Pegasus GC-HRT allowed for quick and easy non-targeted screening of extractables from a common consumer product: the ubiquitous cell phone case. Most components could be identified with high similarity scores against commercial libraries. However, even when faced with low similarity scores against commercial libraries, such as in the case of Biphenol AF, the ability to rely on high mass accuracy allowed for confident identification of components.
Poster
Exploring the Ionization Space in Traditional Electron Ionization with High Resolution GC=TOFMS for a Variety of Compound Classes
-Source temperature was commonly the most significant variable for maximizing molecular ion peak area.
-Chromatographic peak shape was temperature dependant primarily for the non-volatile compounds.
-Ionization conditions were optimized to maximize molecular ion for a variety of compound classes.
-Ionization conditions do change the peak shape and peak area, which relates directly to library searchability.
-Chromatographic peak shape was temperature dependant primarily for the non-volatile compounds.
-Ionization conditions were optimized to maximize molecular ion for a variety of compound classes.
-Ionization conditions do change the peak shape and peak area, which relates directly to library searchability.
Poster
Bioprinted three-dimensional (3D) human liver constructs provide a model for interrogating liver biology
We've designed and constructed a multi-cell type 3D Human Liver Tissue Model using proprietary bioprinting technology. The model contains primary human cell types which maintain form and function using scaffold free self-produced extracellular matrix. The tissue provides an ideal surrogate for human organ specific liver testing for ADME, Toxicology, or disease modeling.
Poster
Utilization of Hydrogen Carrier Gas on a High Resolution GC-TOFMS System: An Application Compendium
GC-HRT methods utilizing hydrogen carrier gas were developed for analysis of representative specialty chemical, forensic, and metabolomic markets.
Poster
Smart Sampling as a fully automated workflow for liquid injection and headspace GC and GC/MS
• To demonstrate a fully automated workflow for both liquid injection and headspace for GC and GC/MS.
• Automatically optimize analysis conditions and derivatization parameters.
• Automate standard preparation and derivatization procedures.
• Reduce analysts time involved in the analysis.
• Compare manual versus automated preparation of standards.
• Automatically optimize analysis conditions and derivatization parameters.
• Automate standard preparation and derivatization procedures.
• Reduce analysts time involved in the analysis.
• Compare manual versus automated preparation of standards.
Poster
Integrated platform including automated bligh and dyer extraction and dual-column
• Automated Bligh and Dyer extraction for metabolomic studies.
• Dual-column UHPLC setup for the analysis of the polar and lipidic fractions.
• Alternating acidic and basic mobile phase for the separation of the polar fraction.
• Identification of unknown compounds by SWATH HR MS2 spectra acquisition.
• Dual-column UHPLC setup for the analysis of the polar and lipidic fractions.
• Alternating acidic and basic mobile phase for the separation of the polar fraction.
• Identification of unknown compounds by SWATH HR MS2 spectra acquisition.
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